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Solid State NMR Spectroscopy for Biopolymers: Principles and Applications
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Catalogue Information
Field name
Details
Dewey Class
572
Title
Solid State NMR Spectroscopy for Biopolymers ([Ebook]) : Principles and Applications / by Hazime Saitô, Isao Ando, Akira Naito.
Author
Saitô, Hazime
Added Personal Name
Ando, Isao
Naito, Akira
Other name(s)
SpringerLink (Online service)
Publication
Dordrecht : Springer , 2006.
Physical Details
: v.: digital
ISBN
9781402043031
Summary Note
Part I Principles 1. Introduction 2. Solid state NMR approach 2.1. CP-MAS and DD-MAS NMR 2.2. Quadrupolar nuclei 3. Brief outline of NMR parameters 3.1. Chemical shifts 3.2. Relaxation parameters 3.3. Dynamics-dependent suppression of peaks 4. Multinuclear approaches 4.1. 31P NMR 4.2. 2H NMR 4.3. 17O NMR 5. Experimental strategies 5.1. Isotope enrichment (labeling) 5.2. Assignment of peaks 5.3. Ultra high-field and ultra high-speed MAS NMR spectroscopy 6. NMR constraints for structural determination 6.1. Orientational constraint 6.2. Interatomic distance 6.3. Torsion angles 6.4. Conformation-dependent 13C chemical shifts 7. Dynamics 7.1. Fast motions with motional frequency >106 Hz 7.2. Intermediate or slow motions with frequency between 106 and 103 Hz 7.3. Very slow motions with frequency < 103 Hz Part II Applications 8. Hydrogen bonded systems 8.1. Hydrogen bond shifts 8.2. 2H quadrupolar coupling constant 9. Fibrous proteins 9.1. Collagen fibrils 9.2. Elastin 9.3. Cerial proteins 9.4. Silk fibroin 9.5. Keratin 9.6. Bacteriophage coat protein 10. Polysaccharides 10.1. Distinction of polymorphs 10.2. Network structure, dynamics and gelation mechanism 11. Polypeptides as new materials 11.1. Liquid crystalline polypeptides 11.2. Blend system 12. Globular proteins 12.1. (Almost) complete assignment of 13C NMR spectra of globular proteins 12.2. 3D structure: ?-spectrin SH3 domain 12.3. Ligand-binding to globular protein 13. Membrane protein I: dynamic picture 13.1. Bacteriorhodopsin 13.2. Phoborhodopsin and its cognitive transducer 13.3. Diacylgycerol kinase 14. Membrane proteins II: 3D structure 14.1. 3D structure of mechanically aligned membrane proteins 14.2. Secondary structure based on distance constraints 15. Biologically active membrane-associated peptides 15.1. Channel-forrming peptides 15.2. Antimicrobial peptides 15.3. Opioid peptides 15.4. Fusion peptides 15.5. Membrane model system 17. Amyloid and related biomolecules 17.1. Amyloid ?-peptide 17.2. Calcitonin (CT):
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Online access to this digital book is restricted to susbcription institutions through IP address (only for SISSA internal users)
Internet Site
http://dx.doi.org/10.1007/1-4020-4303-1
Links to Related Works
Subject References:
Biomaterials
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Biopolymers
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Characterization and Evaluation Materials
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Chemistry, Physical organic
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Materials
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Physical Chemistry
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Polymers
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Solid State Physics and Spectroscopy
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Authors:
Ando, Isao
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Naito, Akira
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Saitô, Hazime
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Corporate Authors:
SpringerLink (Online service)
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Classification:
572
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